10-Hexyl-10H-phenothia­zine-3-carbaldehyde

نویسندگان

  • Hongli Wang
  • Wenyuan Xu
  • Bin Zhang
  • Wenjing Xiao
  • Hong Wu
چکیده

The asymmetric unit of the title compound, C(19)H(21)NOS, contains two mol-ecules, which form dimers via pairs of weak C-H⋯O hydrogen bonds.

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منابع مشابه

10-Ethyl-10H-phenothia­zine-3-carbaldehyde

In the title mol-ecule, C(15)H(13)NOS, the two benzene rings of the tricyclic fused-ring system are inclined at 21.1 (1)°. In the crystal, weak C-H⋯O hydrogen bonds link the mol-ecules into chains along [001]. The crystal packing also exhibits π-π inter-actions with a distance of 3.801 (5) Å between the centroids of the benzene rings of neighbouring mol-ecules.

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The cocrystal 10-(2-methyl-4-phenyl-1H-inden-6-yl)-10H-phenothia­zine–10-(2-methyl-7-phenyl-1H-inden-5-yl)-10H-phenothia­zine (0.54/0.46)

The title compound, 0.535C(28)H(21)NS.0.465C(28)H(21)NS, was synthesized by palladium-catalysed amination. The structure is composed of two isomeric mol-ecules, viz. 10-(2-methyl-4-phenyl-1H-inden-6-yl)-10H-phenothia-zine, and 10-(2-methyl-7-phenyl-1H-inden-5-yl)-10H-phenothia-zine, in the refined ratio 0.535 (12):0.465 (12). The isomers differ by the localization of the double bond in the cycl...

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10-Benzyl-10H-phenothia­zine 9-oxide. Corrigendum

The chemical name of the title compound in the paper by Xu, Sun, Yang & Wang [Acta Cryst. (2009), E65, o1799] is corrected.[This corrects the article DOI: 10.1107/S160053680902577X.].

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10-(Prop-1-yn-1-yl)-10H-phenothia­zine

In the title compound, C(15)H(11)NS, the asymmetric unit comprises one half-mol-ecule; a mirror plane passes through the S atom, the ynamine fragment, the methyl C atom and one methyl H atom. The phenothia-zine moiety has a butterfly conformation and the central six-membered ring has a boat conformation. The dihedral angle between the benzene rings is 149.40 (4)°. The crystal structure is stabi...

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10-(Prop-2-yn­yl)-10H-phenothia­zine

In the mol-ecule of the title compound, C(15)H(11)NS, the butterfly angle between the two planes defined by the two wings of the phenothia-zine unit is 33.5 (8)°. The dihedral angles between the two benzene rings and the propynyl group are 85 (4) and 63 (4)°.

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عنوان ژورنال:

دوره 64  شماره 

صفحات  -

تاریخ انتشار 2008